list_of_ids_plan HZB_MiGo_20231109_BatchX.csv
Create an experimental plan¶
The experimental plan is the core tool to document synthesis.
You should at least have created some processes, eg. wet chemical depositions
as in create_wet_chemical_deposition.md, or cleaning or evaporation.
Or you create a standard sample
as in create_standard_sample.md
Follow the first steps in create_entry.md.
-
Select
HySprint_ExperimentalPlan
as abuilt-in schema
. -
If you have select a
standard sample
by reference (click pen symbol) and clicksave
. This loads the process and information from thestandard sample
in to the experimental plan. -
Enter the
number of substrates
and thesubstrates per subbatch
. It is important that the numbersubstrates per subbatch
devides the numbernumber of substrates
. In a parameter variation there is room fornumber of substrates
devided bysubstrates per subbatch
different variations. So if you hae 8 substrates and 2 substrates per subbatch you have 8/2=4 different parameter variations. Each variation will be applied to the whole subbatch. -
You can now manual change or create the information in
solar cell properties
andplan
.plan
captures the steps planned for the synthesis by reference, if you added astandard sample
you can change the references. -
Parameter variation: for each step you can add some parameter variation. Select a
step
and then add the subsectionparameters
or click thevary parameters
checkbox. If you added aparameters
subsection select a parameter from the drop down menue, eg,quenching/anti_solvent_dropping_time
.
The unit is filled automatically but can be changed. See also set_parameters_in_experimental_plan.md to see how to select the correct parameters. -
Once you entered all variations click the
LOAD STANDARD PROCESSES
button. This copies the information from the template from the reference (or from thestandard sample
) and the parameters subsection into the step As you see, there are now 8/2=4batch processes
. -
Now you can manually change further the parameter by navigating into the
batch process
. Thepresent
checkbox allows you to skip a process for a specific subbatch, just uncheck it if you for example use a buffer layer.!ATTENTION:!
all manually changed data will get lost when pressing theLOAD STANDARD PROCESSES
button again, this will load the template and parameter variation again as specified before. -
If you are happy with the plan click the
CREATE SAMPLES AND PROCESSES
button. This creates all samples, batches, ids and processes. -
This also creates an html overview which you can find in
batch_plan_pdf
. You can download it and open and print it with your browser. This is a summary of all what nomad knows about your experimental plan as well as a reference to the main batch. -
Finally, either navigate to the explore view (see: browse_your_upload.md) and select
HySprint_Batch
and select the one with the ID defined in the experimental plan or follow the reference in the experimental plan. -
Click the
EXPORT BATCH IDS
button and then download thecsv_export_file
.
This looks like this:
0 | 1 | 2 | 3 | 4 | 5 |
---|---|---|---|---|---|
0 | HZB_MiGo_20231109_BatchX_0_0 | Solution and UV standard cleaning | Sam 2PACz spincoating | CsMAFA perovscite spincoating 1 | Evaporation C60, BCP, Cu |
1 | HZB_MiGo_20231109_BatchX_0_1 | Solution and UV standard cleaning | Sam 2PACz spincoating | CsMAFA perovscite spincoating 1 | Evaporation C60, BCP, Cu |
2 | HZB_MiGo_20231109_BatchX_1_0 | Solution and UV standard cleaning | Sam 2PACz spincoating | CsMAFA perovscite spincoating 2 | Evaporation C60, BCP, Cu |
3 | HZB_MiGo_20231109_BatchX_1_1 | Solution and UV standard cleaning | Sam 2PACz spincoating | CsMAFA perovscite spincoating 2 | Evaporation C60, BCP, Cu |
4 | HZB_MiGo_20231109_BatchX_2_0 | Solution and UV standard cleaning | Sam 2PACz spincoating | CsMAFA perovscite spincoating 3 | Evaporation C60, BCP, Cu |
5 | HZB_MiGo_20231109_BatchX_2_1 | Solution and UV standard cleaning | Sam 2PACz spincoating | CsMAFA perovscite spincoating 3 | Evaporation C60, BCP, Cu |
6 | HZB_MiGo_20231109_BatchX_3_0 | Solution and UV standard cleaning | Sam 2PACz spincoating | CsMAFA perovscite spincoating 4 | Evaporation C60, BCP, Cu |
7 | HZB_MiGo_20231109_BatchX_3_1 | Solution and UV standard cleaning | Sam 2PACz spincoating | CsMAFA perovscite spincoating 4 | Evaporation C60, BCP, Cu |
This gives you the ids for the respective parameter variation, which you can then copy into your measurement data (see: upload_measurement.md)