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list_of_ids_plan HZB_MiGo_20231109_BatchX.csv

Create an experimental plan

The experimental plan is the core tool to document synthesis. You should at least have created some processes, eg. wet chemical depositions as in create_wet_chemical_deposition.md, or cleaning or evaporation. Or you create a standard sample as in create_standard_sample.md

Follow the first steps in create_entry.md.

  1. Select HySprint_ExperimentalPlan as a built-in schema.

  2. If you have select a standard sample by reference (click pen symbol) and click save. This loads the process and information from the standard samplein to the experimental plan. grafik

  3. Enter the number of substrates and the substrates per subbatch. It is important that the number substrates per subbatch devides the number number of substrates. In a parameter variation there is room for number of substrates devided by substrates per subbatch different variations. So if you hae 8 substrates and 2 substrates per subbatch you have 8/2=4 different parameter variations. Each variation will be applied to the whole subbatch.

  4. You can now manual change or create the information in solar cell properties and plan. plan captures the steps planned for the synthesis by reference, if you added a standard sample you can change the references.

  5. Parameter variation: for each step you can add some parameter variation. Select a step and then add the subsection parameters or click the vary parameterscheckbox. If you added a parameterssubsection select a parameter from the drop down menue, eg, quenching/anti_solvent_dropping_time.
    grafik
    The unit is filled automatically but can be changed. See also set_parameters_in_experimental_plan.md to see how to select the correct parameters.

  6. Once you entered all variations click the LOAD STANDARD PROCESSES button. This copies the information from the template from the reference (or from the standard sample) and the parameters subsection into the step grafik As you see, there are now 8/2=4 batch processes.

  7. Now you can manually change further the parameter by navigating into the batch process. The present checkbox allows you to skip a process for a specific subbatch, just uncheck it if you for example use a buffer layer. !ATTENTION:! all manually changed data will get lost when pressing the LOAD STANDARD PROCESSES button again, this will load the template and parameter variation again as specified before.

  8. If you are happy with the plan click the CREATE SAMPLES AND PROCESSES button. This creates all samples, batches, ids and processes.

  9. This also creates an html overview which you can find in batch_plan_pdf. You can download it and open and print it with your browser. This is a summary of all what nomad knows about your experimental plan as well as a reference to the main batch.

  10. Finally, either navigate to the explore view (see: browse_your_upload.md) and select HySprint_Batch and select the one with the ID defined in the experimental plan or follow the reference in the experimental plan. grafik

  11. Click the EXPORT BATCH IDS button and then download the csv_export_file. grafik

This looks like this:

0 1 2 3 4 5
0 HZB_MiGo_20231109_BatchX_0_0 Solution and UV standard cleaning Sam 2PACz spincoating CsMAFA perovscite spincoating 1 Evaporation C60, BCP, Cu
1 HZB_MiGo_20231109_BatchX_0_1 Solution and UV standard cleaning Sam 2PACz spincoating CsMAFA perovscite spincoating 1 Evaporation C60, BCP, Cu
2 HZB_MiGo_20231109_BatchX_1_0 Solution and UV standard cleaning Sam 2PACz spincoating CsMAFA perovscite spincoating 2 Evaporation C60, BCP, Cu
3 HZB_MiGo_20231109_BatchX_1_1 Solution and UV standard cleaning Sam 2PACz spincoating CsMAFA perovscite spincoating 2 Evaporation C60, BCP, Cu
4 HZB_MiGo_20231109_BatchX_2_0 Solution and UV standard cleaning Sam 2PACz spincoating CsMAFA perovscite spincoating 3 Evaporation C60, BCP, Cu
5 HZB_MiGo_20231109_BatchX_2_1 Solution and UV standard cleaning Sam 2PACz spincoating CsMAFA perovscite spincoating 3 Evaporation C60, BCP, Cu
6 HZB_MiGo_20231109_BatchX_3_0 Solution and UV standard cleaning Sam 2PACz spincoating CsMAFA perovscite spincoating 4 Evaporation C60, BCP, Cu
7 HZB_MiGo_20231109_BatchX_3_1 Solution and UV standard cleaning Sam 2PACz spincoating CsMAFA perovscite spincoating 4 Evaporation C60, BCP, Cu

This gives you the ids for the respective parameter variation, which you can then copy into your measurement data (see: upload_measurement.md)